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KiloBatcher
Kilo Scale Glass Reactor System
Unlock the potential of kiloscale synthesis with our advanced Glass Reactor System. Engineered to meet the demands of modern laboratories and production facilities, our system offers unparalleled control and versatility.
Advanced Features:
In the kilobatcher, we offer a durable multipurpose glass reactor for bigger volumes, specifically designed for chemical process development in kilo labs, as well as intermediates, surfactants, pigments, API and many more synthesis in compliance with cGMP requirements. Due to the reactor's flame proof and inert materials, solvents and acids can be safely processed in a completely sealed reaction vessel without contaminating the environment.
This versatile reactor system can be easily modified to meet your needs: it comes with interchangeable reaction vessels of range 05 liters to 50 liters, as well as interchangeable stirrers. The glass reactor comes equipped with a lifting device to allow for easy and efficient opening and cleaning.
For chemical processing, we provide complete solutions: Reactor systems with auxiliary equipment such as sampling devices, pH probes, rectification columns with structured packing, process monitoring and control, as well as integrating auxiliary equipment such as temperature control units, nutsche filters / dryers, gas scrubbers or mixing vessels with the reactor system.
Applications Across Industries:
- Various Chemical synthesis
- Multi component reactions
- Extraction / evaporation
- Purification /crystallization
- Distillation / Refluxing
- kilo scale production
- commercial plant scale up activity
Specifications:
- Nominal volume glass vessel ml: 5L, 10L, 20L, 30L and 50L
- Working temperature °C: -20 to + 200 (-60 to + 200)
- Glass reactor made of borosilicate 3.3. Double wall / Triple wall design with bottom drain valve.
- Operating overpressure glass reactor -1 bar or up to +.0.5 bar
- Stainless steel cover plate coated with PFA, 8 opening for solids, feed, liquid dosing, inertisation and others
- Dry running mechanical seal with stirrer drive
- Agitator drive: IKA, Heidolph, Neuation, CAT etc.
- Valve with immersion tube for sampling and draining.
- Immersion tube with temperature sensor Pt100
- Stirring element: gas flushing stirrer or other can be used.
- Heating: double jacket for heat transfer oil
- 4-cornered base chassis, height adjustable via the four adjustable feet
- Lifting lowering device for vessel.
- CIP spray nozzle
- Hose connections (solid and safe) for TCU, optimal temperature control
- Mobile stainless frame on wheels or on feet, fits in standard fume hood
Glass Vessels
The vessels of Labatcher are made of high-quality borosilicate 3.3 glass acc. to ISO 3585, which is chemically and thermally highly resistant. Certainly! Glass vessels used in laboratory scale batch mode glass reactor systems typically have several key features that make them well-suited for various chemical processes and experimentation.
Here are some common features of glass vessels used in these systems:
Borosilicate Glass Construction: Glass vessels are typically made from borosilicate glass, known for its excellent thermal and chemical resistance. This type of glass can withstand a wide range of temperatures and is highly resistant to corrosion from acids, bases, and other reactive substances.
Transparency: One of the primary advantages of glass vessels is their transparency, allowing researchers to visually observe reactions as they occur. This visibility is crucial for monitoring reaction progress, phase changes, and the formation of precipitates or gases.
Versatile Design: Glass vessels come in various shapes and sizes to accommodate different experimental requirements. Common designs include cylindrical, spherical, and flask-shaped vessels, with options for customized configurations based on specific applications.
Temperature Control: Glass vessels are compatible with heating and cooling systems, allowing precise temperature control during reactions. This feature is essential for maintaining optimal reaction conditions and achieving reproducible results.
Stirring Mechanism: Many glass vessels are equipped with integrated stirring mechanisms or ports for attaching stirrers. This ensures thorough mixing of reactants and promotes uniform heat distribution throughout the vessel, enhancing reaction efficiency.
Chemical Inertness: Borosilicate glass is chemically inert, meaning it does not react with most chemicals. This inertness minimizes contamination and ensures the purity of reactions, making glass vessels suitable for a wide range of chemical processes.
Easy Cleaning and Maintenance: Glass vessels are relatively easy to clean and maintain, as they can withstand frequent washing, sterilization, and chemical cleaning procedures without compromising their integrity or performance.
Scalability: Glass vessels used in laboratory scale batch mode reactors are often designed with scalability in mind. This means that the vessel size and configuration can be scaled up for larger production processes while maintaining similar performance characteristics.
Safety Features: Some glass vessels may include safety features such as pressure relief valves, protective coatings, or reinforced designs to prevent breakage and ensure safe operation under varying conditions.
Universal Stirrer Guide
A universal stirrer guide can be used with Glass, Metal and PTFE stirrers’ shaft.
Key Features:
- High level of chemical resistance
- Anti-whip and reduced vibration
- Vacuum (~5mm Hg) and pressure (3-5psi) performance
- No shedding
- Self-releasing joint ring
- Maximum recommended speeds: continuous 500rpm, intermittent 800rpm
Types Of Agitators
Different types and sizes of stirrer are possible based on the type and viscosity of the reaction mass. Available MOC: 1.4435, Combination 1.4435/PTFE or 2.4602 other material are possible on request.
Anchor Stirrer
Two Paddles RCD
Rushton Turbine Stirrer
Propeller Stirrer
Reactor Automation
We can offer complete turnkey solution which includes automation for the reactor system (PC/HMI version.) and integration of third- party instruments i.e. sensors for process parameters, online analytical tools, mass flow controller, pressure controller, dosing pumps & heating cooling system etc. Talk to us to choose optimum degree of automation for labatcher.